Dissertation Process Analytical Technology

In addition, the candidate will present findings at conferences, in scientific publications, and enable industry-wide adaptation of technological advances.

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The event will be held at IMA factory, in Bologna (Italy), on October 23-24, 2018, and is intended to share experience between expert and practitioners. After working through a classical graduate engineering apprenticeship and a few positions in industry, he became the R&D European Group Leader for Kraft Foods in relation to new process automation and processing techniques.

After a few years at Kraft, Martin decided to set up a process automation business called Optimal (syn TQ).

Process Analytical Technology for CO2 Capture, Carbon Dioxide Chemistry, Capture and Oil Recovery, Iyad Karamé, Janah Shaya and Hassan Srour, Intech Open, DOI: 10.5772/intechopen.76176.

The Strategic Analytics group, part of Analytical Development, has an opportunity for a Scientist I/II as a subject matter expert in process analytical technology (PAT).

One of the objectives of this study was to perform a feasibility assessment regarding the development of a NIRS method for end-point determination of the coating process in real time.

Currently, the end-point is estimated by indirect measurements.The calibration is built upon Partial Least Squares regression of NIR spectra and reference values generated by loss on drying on a halogen dryer.It is possible to predict the water content in the calibrated range with a precision comparable to the one of the reference method.An appropriate at-line measurement procedure and a NIR calibration model were established for determination of the actual API content.The calibration is based on time-consuming HPLC reference values, which is the current standard release test.Two distinct models were developed: one focusing on measurements of individual tablets and one using a rotating sample cup as a measuring device, which allows the simultaneous measurement of a larger surface area of several tablets.Principal Component Analysis proves the specificity of both final models for the API.In Project A, fluid bed granulation processes were investigated by in-line particle size measurements using spatial filtering velocimetry and in-line moisture determination by near infrared spectroscopy (NIRS).Implementation of these in-line tools significantly enhanced process understanding during development.In the last section, important regulatory requirements concerning the submission of PAT data and specifics for NIR data are summarised. Process Analytical Technology for CO2 Capture, Carbon Dioxide Chemistry, Capture and Oil Recovery, Iyad Karamé, Janah Shaya and Hassan Srour, Intech Open, DOI: 10.5772/intechopen.76176.


Comments Dissertation Process Analytical Technology

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